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003029

003029-10g



Triethylamine trihydrofluoride


CAS Number: 73602-61-6
   
Molecular Formula: C6H18F3N
   
Molecular Weight: 161.21
   
MDL Number: MFCD00043294

Special Handling and Safety: >1g requires DOT packaging. $20.00 DOT fee applies.

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003029-10g
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003029-25g
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003029-100g
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003029-500g
Regular Price: $169.00
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003029-1Kg
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Purity:98%
Bp:70°/15mm
Density:1.064
Refractive Index:1.3915
 
Pictograms:
Signal Word:Danger
Hazard Statements:H300, H310, H314, H318, H330
Precautionary Statements:P201, P260, P264, P280, P284, P310, P302 + P350, P305 + P351 + P338
UN#:UN2927
Packing Group:I
Hazard Class:6.1
, 8

Flash Point:87°
SDS: See MSDS
 
Excepted Quantities:Max Inner Pack (1g or 1ml) and Max Outer Pack (300g or 300ml)

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A mild and selective fluorinating reagent widely used for nucleophilic substitution, the ring-opening fluorination reaction of epoxide, electrophilic addition, desilylation reaction and so on. Applied in displacement of activated halides to give the corresponding fluorides,1,2 preparation of vicinal difluorides from epoxides,2 synthesis of 3-fluoroazetidine,4 electrochemical fluorodeiodination of alkyl iodides,5 transfluoro-bromination of alkenes in the presence of NBS,6 synthesis of 4-fluorophenols from 4-tert-butylphenols,7 synthesis of perfluorinated primary alcohol adducts with triethylamine as a source of RFO groups in organic syntheses,8 amd synthesis of 9-(2,3-dideoxy-2-fluoro-β-d-threo-pentofuranosyl)adenine (FddA) via a fluorination of 3'-O-benzoyl-5'-O-tritylriboside.9 Also employed as an excellent, selective reagent for cleavage of O-silyl groups in carbohydrates, nucleotides, cyanohydrins.10 

References

1.        J. Fluoine Chem. 2006127, 85.
2.        Tetrahedron 200157, 739.
3.        J. Fluoine Chem. 2005126, 962.
4.        J. Org. Chem. 200671, 7100.
5.        Synlett 2000, 999.
6.        Org. Synth. 199876, 159.
7.        Coll. Czech. Chem. Comm.  200267, 1467.
8.        J. Fluoine Chem. 2002118, 123.
9.        Tetrahedron Lett200142, 2321.
10.        J. Am. Chem. Soc. 1994116, 4697.

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