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M03559

M03559-1g



Triphosgene


CAS Number: 32315-10-9
   
Molecular Formula: C3Cl6O3
   
Molecular Weight: 296.7
   
MDL Number: MFCD00062848

Special Handling and Safety: Over 500g ground shipment and all air shipment Special DOT packaging Charge $20

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M03559-1g
Regular Price: $10.00
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M03559-5g
Regular Price: $12.00
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M03559-10g
Regular Price: $14.00
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M03559-25g
Regular Price: $15.00
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M03559-100g
Regular Price: $30.00
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M03559-500g
Regular Price: $130.00
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M03559-1Kg
Regular Price: $210.00
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Purity:>99%
Bp:203-206°
Mp:79-83°
Density:1.73
 
Pictograms:
Signal Word:Danger
Hazard Statements:H303, H313, H314, H318, H330
Precautionary Statements:P260, P280, P284, P301 + P330 + P331, P303 + P361 + P353, P304 + P340, P305 + P351 + P338, P310, P403 + P233
UN#:UN2928
Packing Group:II
Hazard Class:6.1
, 8

SDS: See MSDS
 
Limited Quantities:100ml (liquid) or 0.5 Kg (solid)
Excepted Quantities:Max Inner Pack (1g or 1ml) and Max Outer Pack (500g or 500ml)

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An efficient carbonylating reagent. A safer substitute for phosgene. Used in the conversion of several amino acids to the corresponding N-carboxyanhydrides,1 synthesis of 3-aryl-1,3-benzoxazine-2,4-diones from anacardic acids,2 preparation of Weinreb amides from carboxylic acids,3 synthesis of direct dyes containing the ureylene group,4 synthesis of quinazolinedione,5 synthesis of azetidin-2-ones,6 debenzylation of tertiary amines,7 and for liquid and solid-phase aza-peptide synthesis.8

1. Tetrahedron Lett. 1988, 29, 5859.
2. Heterocycles 2005, 65, 311.
3. Lett. Org. Chem. 2007, 4, 20.
4. Dyes Pigm. 1996, 32, 193.
5. Synth. Commun. 1991, 21, 285.
6. Tetrahedron 2002, 58, 2215.
7. J. Org. Chem. 2003, 68, 7289.
8. J. Pept. Sci. 1997, 3, 429.

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